Noack Evaporation Loss Tester
ASTM D 5800 - CEC L-40-A-93 - NFT 60161 - DIN 51581-
The Application:
The thermal requirements on
motor oils in particular have risen
considerably over the last few
years. This consequently means
that the testing of these motor
oils and lubricants has nowadays
become more important for reasons
of quality control and operating
safety.
Evaporation losses at high temperatures
generally lead to an increase
in the oil consumption
and additionally cause a detrimental
change in the lubrication
properties of the oils.
The Test Method
The test method is standardized
in DIN 51581, CEC L-40-A-93
and ASTM D 5800. The oil sample
is heated in a testing device,
the evaporation crucible, and
subsequently re tained at the
testing temperature for exactly
60 minutes. Whilst the testing
temperatures can generally be
as high as 400°C, motor oils are
usually tested at 250°C ±0.5°C
.
A constant flow of air, brought
about by a differential pressure,
extracts the resultant oil vapours.
The airflow is accurately regulated
by the integrated digital pressure
controller. It can be read-off
using an inclined manometer.
According to CEC specifications,
the partial pressure should be
equal to 20 mm water column(
1.96 mbar).
The evaporation crucible with the
oil sample is weighed before and
after the heating process. The
evaporation loss is then calculated
from the resultant weight
difference and is expressed in
percentage by mass.
The Technology
The temperature control of the
evaporation tester VP250 is carried
out by a PID microprocessor
controller. This control technique
results in high level of reproducibility
and repeatability of the test
results. The limits quoted in DIN
51581, ASTM D5800/a and CEC
L-40-A-93 can be easily observed
with large safety margins.
Features
- Vacuum pump with oil filter
- Port to document the temperature
and pressure course
- Microprocessor-controlled
temperature control unit
⇒ high control accuracy
⇒ automatic adaptation of the
control parameters
- Wide temperature range from
150 to 300°C
- ⇒ also suitable for special lubricants
(gear lubricant oil)
- PT100 probe calibrated
against gauged mercury
thermometer with 0.1°C scale
⇒ deviation to real temperature
is smaller than 0.5°C
- Excess temperature protection
- LCD display for actualt temperature
/ pressure and test
time
- Timer with acoustic signal
⇒ no separate stopwatch
required
- Faults are displayed acoustically
and visually
⇒ no measurement errors
- Automatic sensor adjustment;
⇒ no long-term drift
- Equipped with differential pressure controller to control auto
matically differential pressure;
Standard set pressure: 20 mm H2O; long-term stabi
lised pressure sensor; tolerance extent ± 1%;
Vacuum pump with air filter.
Accessories
The following accessories are available:
- Glassware set consisting of two 2 litre Woulf bottles,
glass delivery tubes and silicon hoses.
- Stable supporting unit including an inclined tube
manometer 0-30 mm H2O
⇒ provide correct positioning of glass bottles
⇒ reading and manually controlling of pressure
- Two officially gauged thermometers and a thermo
meter holder
- Reference oil for testing the system
- Balance, range 2000 g; accuracy 0.01g
- Cooling unit for cooling down the evaporation
crucible after the test
⇒ increases reproducibility
⇒ provides safe cooling down method as
- ⇒ awkward splashing of water is thus avoided
Technical Specifications
- Mains Connection 230V 110V
(selectable)±10%
50/60 Hz, 1300 VA
- Heating power 950 VA at 250°C
- Pressure range: up to 21 mmWS
- Accuracy: ± 0,2°C /
± 0,02 mmWS
- Temperature Range 150.0°C to 300.0°C
- Temperature Display LCD, resolution 0.1°C
- Temperature Setting menu controlled,
- Time Displays, • for test time
- Separate Timer 60 min. countdown
display can be called
up
- Type of Control digital PID-control
- Control Accuracy ±0.1°C at 250°C
- Temperature Sensors Pt100 (display / control)
- Port: TTL
- Excess Temperature independent safety circuit
Protection with separate sensor,
Warning Signal acoustic
Alarm Signal for excess temperature:
for faults: acoustic and shown
on display
- Dimensions, WxHxD 278x316x300 mm
- Weight (net/gross) 18 kg / 23 kg
Standard Equipment
Vacuum pump; evaporation crucible;
tools, test balls, nozzle cleaner; crucible holder,
cleaning brush, protective gloves;
300g Wood metal
Each instrument is actually tested in the production facilities and is provided with a quality control report which includes pressure/temperature curve according to standard requirements.
To avoid operator's attendance, an automated vacuum controller is recommended. This option can also be installed on previous generation instruments.
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